Synthesis and characterization of N,N'-carbonyl difatty amides from palm oil.

نویسندگان

  • Emad A Jaffar Al-Mulla
  • Wan Md Zin Wan Yunus
  • Nor Azowa Bt Ibrahim
  • Mohd Zaki A Rahman
چکیده

N,N'-Carbonyl difatty amides (CDFAs) have been synthesized from palm oil using sodium ethoxide as catalyst. Ethyl fatty esters (EFEs) were produced as a by-product as well as glycerol. The synthesis was carried out by reflux palm oil and urea in presence of ethanol. In this process, palm oil gave 79% pure CDFAs after 8 hours and molar ratio of urea to palm oil was 6.2: 1 at 78 degrees C. Both CDFAs and EFEs have been characterized using elemental analysis, Fourier transform infrared (FTIR) spectroscopy and (1)H nuclear magnetic resonance (NMR) technique.

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عنوان ژورنال:
  • Journal of oleo science

دوره 58 9  شماره 

صفحات  -

تاریخ انتشار 2009